鸭绿江学术资源论坛's Archiver

leeb 发表于 2007-8-23 16:29

求助专利一篇

好像是篇日本专利,我只有这么一点信息:JP 63-89501
做实验急用,请高手帮忙。万份感谢!

chenwei6669 发表于 2007-8-24 09:01

找了好久,却看不了原文,只有摘要.

Abstract of JP63089501

PURPOSE:To produce industrially pectic acid by selectively converting methoxycarbonyl groups of the side chains of pectin into carboxyl groups without causing degradation of the chemical structure of its main chain, by saponifying pectin under specified reaction conditions and treating the saponificate with an acid. CONSTITUTION:Powered or slurried pectin is saponified at a about -2-10 deg.C in the presence of about 0.8-1.6mol, per mol of uronic acid residues of pectin, of an alkali (preferably, NaOH or KOH) in a lower alcohol such as an about 40-90wt% aqueous alcohol solution (preferably, a lower alcohol such as methanol), and the obtained saponificate is treated with an acid (e.g., hydrochloric acid or sulfuric acid). According to the above process, pectic acid can be produced as a result of the selective conversion of methoxycarbonyl groups of the side chains of pectin into carboxyl groups without causing undesirable side reactions such as cleavage of the main chain of a pectin molecule. Further, this process can provide a highly pure product because impurities adsorbed by the pectin powder can be easily removed during said treatment and is industrially advantageous because masstreatment is easy.

leeb 发表于 2007-8-24 11:22

谢谢chenwei6669,虽然只是摘要,总还是有些帮助的。再次感谢!

页: [1]

Powered by Discuz! Archiver 6.1.0  © 2001-2007 Comsenz Inc.